Best one I've seen to date is "Schematron" from O'Reilly Media available in electronic (Adobe PDF) format for $9.99 USD. Provides a great overview and set of examples using Schematron, albeit exclusively in hierarchically linked XML documents. It does assume the reader already has a strong understanding of XML and XSLT. If you are a bit rusty on XSLT or XQuery, you'll want to pick up a book on that as well.
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